Laboratry of analytical methods 4.006
Cryomagnetic system for Mössbauer spectroscopy in external magnetic fields (IFMS) CRYOGENIC LIMITED
Available services/measurements:
- Sample measurements in temperature range of 1.7–300 K
- Sample measurements in a magnetic field of 0–7 T
X-ray diffractometer BRUKER D8
Available services/measurements:
- Measurements of diffraction for powdered materials and thin layers (qualitative a quantitative phase analysis)
- Measurements of texture
- Internal stress measurements
- Reflectivity measurements
- Point measurements - diameter 100 μm
- Measurements in a temperature range 20–900 °C using different reaction atmospheres
Special equipment
- Three-axis cradle
- Platform allowing a 3-degree of freedom sample movement
- Automatic sample exchange
- Reaction chamber allowing measurements in wide temperature range and under various pressures and atmospheres
Adsorption analyser Autosorb iQ
Available services/measurements:
- Measurements of specific surface area
- Determination of sample porosity in a pore range of 0.4 to 50 nm
- Determination of active sites and their dispersion of a catalyst
- Temperature programmable reduction, oxidation, desorption
- Drying and outgassing of samples
Arc furnace SP-MP20-7
Available services/measurements:
- Melting of metals at temperatures up to 3000 °C under both low- or high-pressure atm
- Preparation of alloys with weight < 10 g
Glove box - JACOMEX
Available services:
- Performing tasks under inert atmosphere with the help of 4 gloves
- Connected to a nitrogen gas generator (purity > 99.9995%)
Furnaces
- Tube furnace (temperatures up to 1200 °C)
- Rotary tube furnace temperatures up to 1100 °C, inert working atm. – nitrogen, argon)
Measurement stations
High-powered PCs with additional measurement and control cards
Other equipment (high-voltage sources, digital oscilloscopes, function generators)
Analytical balance RADWAG - AS 310.3Y
- Maximum weight – 310 g
- Resolution – 0.1 mg
